2012, 32(5):452-457.

WSe2纳米结构的合成及减摩性能研究

1.?

吉林师范大学 功能材料物理与化学教育部重点实验室,吉林 四平 136000

2.?

江苏大学 江苏省材料摩擦学重点实验室,江苏 镇江 212013

通讯作者: 杨景海, liuyanqing@jlnu.edu.cn

收稿日期: 2012-05-21

基金项目: The project was supported by the National Natural Science Foundation of China(61178074), Science and Technology Development Project of Jilin Province(201115218) and Natural Science Foundation of Jilin Province (BK2010348).
国家自然科学基金项目(61178074)、吉林省科技发展计划项目(201115218)和江苏省自然科学基金项目(BK2010348)资助.

Synthesis and Frictional Properties of WSe2 Nanostructures

1.?

Key Laboratory of Functional Materials Physics and Chemistry of the Ministry of Education, Jilin Normal University, Siping 136000, China

2.?

Jiangsu University,Key Laboratory of Materials Friction and Wear of Jiangsu Province,Zhenjiang 212013,China

Corresponding author: YANG Jing-hai, liuyanqing@jlnu.edu.cn

Received Date: 21 May 2012

引用本文: 刘艳清, 张静, 吴钰涵, 李长生, 阎永胜, 杨景海. WSe2纳米结构的合成及减摩性能研究[J]. 摩擦学学报, 2012, 32(5): 452-457.

Citation: LIU Yan-qing, ZHANG Jing, WU Yu-han, LI Chang-sheng, YAN Yong-sheng and YANG Jing-hai. Synthesis and Frictional Properties of WSe2 Nanostructures[J]. TRIBOLOGY, 2012, 32(5): 452-457.

将W粉和Se粉按一定比例混合,直接密封在石英管中加热或高能球磨、压片,在Ar气氛中加热,得到了不同形貌的WSe2纳米结构.利用X射线衍射仪(XRD)、扫描电子显微镜(SEM)和透射电子显微镜(TEM、HRTEM)分析了WSe2纳米结构的组成、微观形貌和组织形态;利用UMT-2摩擦试验机考察了WSe2作为HVI500液体基础油添加剂的摩擦磨损性能.研究结果表明:直接密封加热得到的产物为棒状WSe2纳米材料,最小棒直径为6 nm;球磨、压片后加热得到WSe2纳米颗粒,颗粒的平均尺寸在50 nm以下,二者都具有层状结构和良好的结晶性.添加质量分数5%的WSe2纳米材料作为基础油添加剂能够显着降低摩擦系数,减少磨损,增强了材料抗疲劳磨损能力.

关键词: 固相反应, WSe2纳米结构, 润滑油添加剂, 摩擦, 磨损
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    WSe2纳米结构的合成及减摩性能研究

    刘艳清, 张静, 吴钰涵, 李长生, 阎永胜, 杨景海